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Journal of the American Chemical Society

Justus Liebig's Annalen der Chemie.

GA Prochazka

文献索引:Scholl; Donat Justus Liebigs Annalen der Chemie, 1934 , vol. 512, p. 1,21 Full Text Show Details Vaughan et al. Journal of the American Chemical Society, 1954 , vol. 76, p. 1748,1751

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被引用次数: 1

摘要

Methods for the preparation of the mononitrosalicylic acids.(1) 50 grns of nitric acid (1.5 sp. gr.) are added in small portions to a cold solation of 100 gms salicylic acid in 500 or 800 gins glacial acetic acid. The resulting liquid i 4 diluted with 2 or: j vol. water and cooled down very low.(2) 10 gms salicylic acid are gradually added to a mixture of 10 gms fuming nitric and 10 or 12 gnis glacial acetic. acid; the resulting liquid is poured in 250 cc very cold water. The ...