Bulletin of the Chemical Society of Japan

The New Synthetic Method of β-Acetyl-butyrolactone

Y Nishizawa

文献索引：Nishizawa Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 1282

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摘要

After the oil was dissolved completely, the aqueous solution was neutralized with 30% sulfuric acid to pH 8.8. 2 and then 20 g. of sodium bicarbonate and 54ml. of 37% formaline were added. After the mixture was allowed to stand overnight at room temperature, acidified with 30% sulfuric acid and extracted continuously with ether. The ether layer was dried with anhydrous sodium sulfate and then ether was evaporated. The residual oil was distillated ...