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The Journal of Organic Chemistry

Synthesis of simple hydrazones of carbonyl compounds by an exchange reaction

GR Newkome, DL Fishel

文献索引:Newkome,G.R.; Fishel,D.L. Journal of Organic Chemistry, 1966 , vol. 31, p. 677 - 681

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被引用次数: 83

摘要

Simple X-unsubstituted hydrazones of most aldehydes or ketones, usually difficult to obtain in good yields and high purity, may be so prepared from the corresponding N, N- dimethylhydrazones by exchange with anhydrous hydrazine. Since azine formation is nil under these conditions, the reaction can be followed by observing loss of color. The