New Journal of Chemistry

… electrochemical observation of the 17-electron ruthenocenium cation in fluorinated ruthenocene-containing β-diketones; polymorphism of C 10 H 21 and C 10 F 21 …

E Erasmus, JC Swarts

文献索引：Erasmus, Elizabeth; Swarts, Jannie C. New Journal of Chemistry, 2013 , vol. 37, # 9 p. 2862 - 2873

被引用次数: 8

摘要

Ruthenocene-containing β-diketones, RcCOCH2COR with Rc= ruthenocenyl and R= C10F21 (1), CF3 (2), C6F5 (3), C10H21 (4), CH3 (5) and C6H5 (6), were synthesised by Claisen condensation of the appropriate methyl ester with acetylruthenocene, and their spectroscopic, electrochemical and thermal properties were compared. A new synthetic route utilising 1, 2, 3-benzotriazol-1-ylethanone (9) or 1, 2, 3-benzotriazol-1-yl ( ...

~95%

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