2-(Diethylamino) ethanethiol, a new reagent for the odorless deprotection of aromatic methyl ethers

J Magano, MH Chen, JD Clark…

文献索引：Journal of Organic Chemistry, , vol. 71, # 18 p. 7103 - 7105

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被引用次数: 42

摘要

... The Journal of Organic ... The aqueous phase was extracted with ethyl acetate (3 × 25 mL), and the combined organic extracts were washed with water (3 × 10 mL) and saturated ... 1221, 821, 754 cm - 1 . 1 H NMR (CDCl 3 , 400 MHz): δ 11.46 (s, 1 H), 8.22−8.24 (d, 1 H, J = 7.99 Hz ...