A study of the acid-catalyzed reaction of N-bromosuccinimide in methanol with some. alpha.,. beta.-unsaturated carbonyl compounds

…, TG Aucoin, DE Gipe, DF Shellhamer

文献索引：Heasley, Victor L.; Wade, Kimberley E.; Aucoin, Thomas G.; Gipe, Daphne E.; Shellhamer Dale F.; Heasley, Gene E. Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1377 - 1379

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被引用次数: 23

摘要

Method C. Solutions were prepared by sequential addition of 2.5 X lo-'mol quantities of pyridine 1-oxide, trimethylsilanecarbonitrile, and acylating agent to 0.4 mL of chloroform-d that contained 1% tetramethylsilane. The final solutions were approximately 0.5 M in each reactant. NMR tubes with screwcaps and Teflon liners (Wilmad No. 507-TR) were used as reaction vessels.