Synthesis

A simple and facile carboxylation method and its application for synthesis of liquid crystals

ASY Lee, CC Wu, LS Lin, HF Hsu

文献索引：Lee, Adam Shih-Yuan; Wu, Chih-Chiang; Lin, Li-Shin; Hsu, Hsiu-Fu Synthesis, 2004 , # 4 p. 568 - 572

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被引用次数: 0

摘要

Abstract Sonication of a mixture of magnesium powder, 1, 2-dibromoethane, aryl bromide and diethyl dicarbonate in THF followed by treatment with BF 3· OEt 2 at room temperature afforded aryl ester with reasonable yield. A series of aryl bromides were investigated and transformed to their corresponding aryl esters under the reaction conditions.