Journal of the American Chemical Society

Heterocycles Containing p-Phenylene Units. III. Substituted Amines

RC Fuson, HO House

文献索引：Fuson; House Journal of the American Chemical Society, 1953 , vol. 75, p. 5744

全文：HTML全文

被引用次数: 3

摘要

40.2 g. of#-phenylsulfonamidotoluene,'22.0 g. of hexamethylene bromide, 75.0 g. of anhydrous potassium carbonate and 300 ml. of acetone was boiled under reflux, with stirring, for 2 hours. After three-fourths of the acetone had been distilled from the reaction mixture, the residue was poured into 1 1. of water. The oily product, which partially solidified when allowed to stand, was filtered. An attempted crystallization of the solid from ethanol ...