Helvetica chimica acta

Synthesis and NMR spectroscopic investigation of a macrocyclic diphosphine ligand and its nickel (II) and palladium (II) complexes

M Widhalm, H Kalchhauser, H Kählig

文献索引：Widhalm; Kalchhauser; Kahlig Helvetica Chimica Acta, 1994 , vol. 77, # 1 p. 409 - 418

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被引用次数: 14

摘要

Abstract The preparation of a macrocyclic diphosphine ligand 5 incorporating a binaphthyl unit and its Ni II and Pd II complexes, 6 and 7, is described. A complete assignment of 1 H,- 13 C-, and 31 P-NMR data on the basis of 2D NMR spectroscopy (1 H, 1 H-, 13 C, 1 H-, 31