A convenient synthesis of O-ethyl-1-aminoalkylphosphinates

T Gajda

文献索引：Gajda, Tadeusz Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 85, # 1-4 p. 59 - 64

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被引用次数: 24

摘要

Abstract 1-Aminoalkylphosphinates 4 have been obtained in good yields in a one-step transformation by the Mitsunobu reaction of 1-hydroxyalkylphosphinates 1 with hydrazoic acid, and subsequent treatment of the intermediate azides 2, with triphenylphosphine, followed by hydrolysis of the iminophosphoranes 3 with water.