Structures of racemic monofluoro-substituted mandelic acids, their relation to the thermochemical properties and an analysis of short intermolecular fluorine–carbon …

S Larsen, K Marthi

文献索引：Larsen, Sine; Marthi, Katalin Acta Crystallographica, Section B: Structural Science, 1994 , vol. 50, # 3 p. 373 - 381

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被引用次数: 14

摘要

V=1509.9 (6) A3, Z=8, D,.=l.497gcm-3 #= 10.92 cm-~, F(000) = 704, R = 0.048 for 2977 contri- buting reflections, mp 368.4 (5)K. p-Fluoroman- delic acid, orthorhombic, Pbca, a = 9.4685 (9), b = 16.497 (2), c = 9.7677 (8) A, V= 1525.7 (5) ,~3 Z= 8, Dx = 1.481 gcm-3,/x = 10.80cm-~, F(000)= 704, R = 0.042 for 1489 contributing reflections, mp 408.9 (5)K. The results obtained from the structure determination are related to their physico-chemical properties ...