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Tetrahedron

Nouvelle voie d'accés en une étape au squelette de la benzo [g] indole [2, 3a] indolizinone-5: Etude structurale en RMN 2D

M Laguerre, C Boyer, M Atfani

文献索引:Laguerre, M.; Boyer, C.; Atfani, M. Tetrahedron, 1988 , vol. 44, # 23 p. 7109 - 7118

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被引用次数: 3

摘要

A one pot synthesis of benzo [g] indolo [2, 3-a] indolizinone-5 is described. Starting from tryptamine hydrochloride and methyl o-phthalaldehydic acid ester, 85% yield is obtained in refluxing n-butanol. In spite of differences with published data, the structure of final compound has been firmly established by 2D heteronuclear correlation NMR spectroscopy.