The Journal of Organic Chemistry

Notes. 1, 1, 5-Trichloro-1, 3-pentadiene from the Pyrolysis of 5, 5, 5-Trichloro-4-acetoxy-1-pentene.

K McMichael, R Clement

文献索引：McMichael,K.D.; Clement,R.A. Journal of Organic Chemistry, 1961 , vol. 26, p. 585 - 587

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被引用次数: 1

摘要

and Sons, Inc., New York, NY, 1956, p. 212. sure waa then reduced and 5, 5, btrichloro-4- acetoxy-l-pentene (JI)(73 g., 92%) was collected as a colorlees liquid, bp 96-97'(16mm.), ny 1.4694 [lit. Bb. p. 97-98'(16 mm.), nD 1.46981. In the infrared (sodium chloride sandwich), this material exhibited absorption, among others, at 1750 (ester carbonyl), 1637 (unsaturation), and 992 and 922 (terminal methylene) em.-1 1, l, 6-T~ ch. Z 0 r+ ll~ p~~( ...