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Arene-perfluoroarene interactions in crystal engineering: structural preferences in polyfluorinated tolans

…, C Dai, AJ Scott, S Borwick, AS Batsanov…

文献索引:Smith, Caroline E.; Smith, Philip S.; Thomas, Rhodri Ll.; Robins, Edward G.; Collings, Jonathan C.; Dai, Chaoyang; Scott, Andrew J.; Borwick, Simon; Batsanov, Andrei S.; Watt, Stephen W.; Clark, Stewart J.; Viney, Christopher; Howard, Judith A. K.; William, Clegg; Marder, Todd B. Journal of Materials Chemistry, 2004 , vol. 14, # 3 p. 413 - 420

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被引用次数: 83

摘要

The compounds 4-ROC6F4CCPh (4) where R= Me (a), Et (b), Prn (c), Pri (d), Bun (e), n- C5H11 (f), PhCH2 (g), PhCH2CH2 (h), 4-MeC6H4 (i), 4-EtC6H4 (j) and menthyl (k), have been prepared by reaction of C6F5CCPh (3) with ROH in the presence of KOH, and characterised by NMR (1H, 13C, 19F) and mass spectroscopy. The single-crystal structures of PhCCPh· C6F5CCC6F5 (1∶ 2), 3 and 4a, c, d, f, g, i have been determined by X-ray ...