Condensation of 1, 4-diacetyl-2, 5-piperazinedione with aldehydes promoted by ultrasonically dispersed potassium

LX Wang, YZ Shi, MH Xu, HW Hu

文献索引：Wang, Li Xin; Shi, Yao Zeng; Xu, Ming Hua; Hu, Hong Wen Organic Preparations and Procedures International, 1996 , vol. 28, # 2 p. 226 - 230

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被引用次数: 7

摘要

Volume 28, No. 2, 1996 OPPI BRIEFS reagent"! The derivatives of DAPDO (1) have great potential in biochemistry* and synthesis9 and may be obtained by the condensation of aldehydes with piperazinedione (PD0)'O or with DAPDO using strong bases (eg t-BuOK)," by the use of phosphorus ylide, I2 by microwave irradiation'> or using phase-transfer~ atalysis'~ in a few hours to a few days in moderate to excellent yields; however, there ...