前往化源商城

THE ACETYLATION OF ORTHO-HYDROXY ALDEHYDES

T Malkin, M Nierenstein

文献索引:Malkin; Nierenstein Journal of the American Chemical Society, 1931 , vol. 53, p. 239

全文:HTML全文

被引用次数: 10

摘要

/OCOCHa Y\CH CHaCOO \OCOCHs CHsCOO I I1 ... In the present communication, a method for the preparation of triacetyl- phloroglucin aldehyde (11) is described, and this method has also been ex- tended to the preparation of diacetyl-8-resorcylic aldehyde and acetyl- salicylic aldehyde. All these aldehydes are smoothly acetylated in ethereal solution with acetic anhydride and anhydrous potassium carbonate in which manner all rise of temperature is controlled. ...