Development of a preparative-scale asymmetric synthesis of (R)-p-tolyl methyl sulfoxide for use in a one-pot synthesis of a drug intermediate containing a …

Z Han, JJ Song, NK Yee, Y Xu, W Tang…

文献索引：Pedrosa, Rafael; Sayalero, Sonia; Vicente, Martina; Maestro, Alicia Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 2177 - 2180

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被引用次数: 14

摘要

... Select a Journal or Book ... 13 C NMR (CDCl 3 ) δ 158.3, 155.93, 154.1, 142.2, 140.3, 137.04, 136.9, 130.2, 126.5 (q, J = 286 Hz), 123.9, 115.5, 115.3 ... The organic solvents were removed, and the residue was diluted with heptane (100 mL) and EtOAc (20 mL) and loaded onto a ...