Abstract Three siloxanediols HO (CH 2) n [Si (CH 3) 2 O] x Si (CH 3) 2 (CH 2) n OH (n= 3, x= 2, 3 and n= 11, x= 1) have been prepared from the corresponding silicon hydrides, and characterized by 13 C and 29 Si NMR spectroscopy. The thermal behaviour of several oligosiloxanes containing hydroxyalkyl groups has been studied by differential scanning calorimetry (DSC) in the temperature range− 173 to 37 C.
[Lee, Soonho; Jeon, Youngtae; Lim, Youngdon; Cho, Younggil; Lee, Sangyoung; Kim, Whangi Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2583 - 2588]