The Journal of Organic Chemistry

A new route to acetylenes

DP Bauer, RS Macomber

文献索引：Bauer,D.P.; Macomber,R.S. Journal of Organic Chemistry, 1976 , vol. 41, p. 2640 - 2642

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被引用次数: 13

摘要

Decomposition of Aryldiazonium Fluoroborate (1). General Procedure. The salt (0.01 mol) was dissolved in acetone (30 ml). To the solution was fir& added CSz (30 ml) and then NaI (1.5 g) in small quantities under stirring. After nitrogen evolution the mixture was refluxed for 30 min and the solveqt evaporated. The crude was dissolved in chloroform, washed with water and dried and the solvent removed under vacuum. The mixture was analyzed on ...