Limitations on the Persistence of Iminoxyls: Isolation of tert-Butyl 1, 1-Diethylpropyl Ketiminoxyl and Related Radicals

BM Eisenhauer, M Wang, H Labaziewicz…

文献索引：Journal of Organic Chemistry, , vol. 62, # 7 p. 2050 - 2053

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被引用次数: 21

摘要

... The Journal of Organic ... 1047, 1010, 992, 923, 856, 808 cm - 1 . 1 H-NMR δ 0.70(t, 9H, J = 7.6 Hz), 1.212 (s, 9H), 1.67 (q, 6H, J = 7.4 Hz). ... The organic product was extracted with ether, dried (Na 2 SO 4 ), and concentrated to the pale green bis-imine (1.24 g, 76%, IR 1594 cm - 1 ...