Organic letters

Synthesis of the Naphthalene Portion of the Rubromycins

X Xie, MC Kozlowski

文献索引：Organic letters, , vol. 3, # 17 p. 2661 - 2663

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被引用次数: 54

摘要

... Volume: Page: ... Organic Letters. ... a (a) (i) Br 2 , AcOH, (ii) NaH, BnBr; 86%; (b) (i) mCPBA, (ii) KOH, (iii) NaH, BnBr; 61%; (c) (i) nBuLi, (ii) Cr(CO) 6 , (iii) Me 3 OBF 4 ; 60−90%; (d) THF, Ac 2 O, 53%; (e) TBAF, THF, 31%; (f) PPTS, (MeO) 2 CMe 2 ; (g) PPTS, acetone. ...