4154 J. Org. Chem., Vol. 43, No. 21, 1978 Taylor and Wachsen chloride. The resulting suspension was kept at room temperature for 12 h. Filtration and concentration left a syrup which crystallized on scratching. The solid was suspended in water, filtered, and recrystallized from acetonehexane giving colorless crystals. The N-benzoyl-N'- oxamoylureas 12c, 12d and 12f were prepared following procedures similar to the one ...