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Prototypical phosphorus analogues of ethane: General and versatile synthetic approaches to hexaalkylated PP diphosphonium cations

JJ Weigand, SD Riegel, N Burford…

文献索引:McFarlane, H. Christina E.; McFarlane, William; Nash, John A. Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , # 1 p. 240 - 244

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被引用次数: 42

摘要

... Select a Journal or Book. ... NMR: Bruker AVANCE 500 ( 1 H (500.13 MHz), 13 C (125.76 MHz) chemical shift referenced to δ TMS = 0.00; 31 P (202.46 ... General Procedure for the Preparation of Phosphinophosphonium Salts [R 3 P−PR' 2 ][OTf] (6a−e[OTf]): Me 3 SiOTf (180 μL ...