The reaction of red phosphorus with 1??bromonaphthalene in the KOH–DMSO system: Synthesis of tri (1??naphthyl) phosphane

…, TI Vakul'skaya, SS Khutsishvili…

文献索引：Kuimov, Vladimir A.; Malysheva, Svetlana F.; Gusarova, Nina K.; Vakul'Skaya, Tamara I.; Khutsishvili, Spartak S.; Trofimov, Boris A. Heteroatom Chemistry, 2011 , vol. 22, # 2 p. 198 - 203

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被引用次数: 9

摘要

Abstract Red phosphorus reacts with 1-bromonaphthalene in the KOH–DMSO system upon heating (47–70 C, 3 h) to give tri (1-naphthyl) phosphane in 10% yield. Microwave activation (600 W, 6 min) of the reaction affords the above-mentioned phosphane in 25% yield.© 2011 Wiley Periodicals, Inc. Heteroatom Chem 22: 198–203, 2011; View this article online at wileyonlinelibrary. com. DOI 10.1002/hc. 20671