Large-scale preparation of 2-methyloxazole-4-carboxaldehyde

GE Benoit, JS Carey, AM Chapman…

文献索引：Organic Process Research and Development, , vol. 12, # 1 p. 88 - 95

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被引用次数: 13

摘要

... This procedure was scaled up to a 75 kg input scale, and the product was obtained in 74 ... would lead to the partial formation of aminal 17 later in the process (Figure 2 ... To remove the residual sodium hydrogen sulfate and acetic acid entrained within the organic layer a wash with ...