Journal of fluorine chemistry

N-fluoro-bis (trifluoromethanesulfonyl) imide. An improved synthesis

DD Desmarteau, M Witz

文献索引：Desmarteau, Darryl D.; Witz, Michael Journal of Fluorine Chemistry, 1991 , vol. 52, # 1 p. 7 - 12

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被引用次数: 67

摘要

An improved synthesis of (CF 3 SO 2 ) 2 NH and its conversion to the very useful fluorination reagent (CF 3 SO 2 ) 2 NF is described. The five-step synthesis yields (CF 3 SO 2 ) 2 NF in 76% yield based on the starting CF 3 SO 2 F. ... Journal of Fluorine Chemistry, 52 (1991) 7-12 N-FLUORO-BIS(TRIFLUOROMETHANESULFONYL) IMIDE. AN IMPROVED SYNTHESIS DARRYL D. DESMARTEAU* AND MICHAEL WITZ Howard L. Hunter Chemistry Laboratory, ...