THE SYNTHESIS OF ALPHA, BETA-UNSATURATED ETHERS

WM Lauer, MA Spielman

文献索引：Lauer; Spielman Journal of the American Chemical Society, 1931 , vol. 53, p. 1535

全文：HTML全文

被引用次数: 12

摘要

A. Preparation of the Chloro Ethers. Equation (l).-The procedure followed was essentially that described by Boord. In working with propionaldehyde or butyraldehyde, however, greater care was necessary. When the aldehyde and alcohol were mixed, considerable heat was evolved, and if thorough cooling with an ice-salt bath was not effected before the influx of the hydrogen chloride, unmanageable colored liquids were obtained from which none ...