Tetrahedron letters

Reaction of β-fluorovinamidinium salt with Grignard reagents. Facile and efficient route to (Z)-α-fluoro-α, β-unsaturated aldehydes

H Yamanaka, Y Odani, T Ishihara, JT Gupton

文献索引：Yamanaka, Hiroki; Odani, Yasumasa; Ishihara, Takashi; Gupton, John T. Tetrahedron Letters, 1998 , vol. 39, # 38 p. 6943 - 6946

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被引用次数: 10

摘要

Download full text in PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... Kase K, Katayama M, Ishihara T, Yamanaka H, Gupton JT. J. Fluorine Chem. in press. ... (Z)-2-Fluoro-3-phenyl-2-propenal (3a): mp 46–47 °C. IR (KBr): 1688, 1634 cm −1 . 1 H NMR (CDCl 3 , TMS): δ 6.63 (d, J=34.3 Hz, 1H), 7.42–7.51 (m, 5H), 9.35 (d, J=17.1 1H). 19 F ...