Synthesis and Spectral Studies (FT??IR, 1H, 13C, 119Sn, and Mass Spectrometry) of Mixed Organotin (IV) Compounds Containing a Long Chain Alkyl Group (n?? …
Sadiq??ur??Rehman, S Ali, A Badshah
文献索引：Sadiq-ur-Rehman; Ali, Saqib; Badshah, Amin Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 2004 , vol. 34, # 3 p. 443 - 457
Abstract Di??and triorganotin (IV) compounds of the type R2SnR2′ and R3SnR′(R= CH3, n??C4H9, C6H5, C6H5CH2 and R′= n??C7H15) have been prepared by the reaction of R2SnCl2 and R3SnCl with a stoichiometric amount of n??heptylmagnesium bromide, prepared in situ in dry diethyl ether. The products obtained were vacuum distilled. The structural assignments were made on the basis of spectral studies such as FT??IR, 1H, 13C ...
