Photochemical cyclization of 2-alkyl-3-aryl-2-cyclohexenones and 2-alkoxy-3-aryl-2-cyclohexenones

A Feigenbaum, Y Fort, JP Pete…

文献索引：Feigenbaum, Alexandre; Fort, Yves; Pete, Jean-Pierre; Scholler, Denise Journal of Organic Chemistry, 1986 , vol. 51, # 23 p. 4424 - 4432

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被引用次数: 18

摘要

Anal. Calcd for CllH15N304: C, 52.17; H, 5.97; N, 16.59. Found: C, 52.24; H, 5.93; N, 16.56. 2,3'-(P heny1imino)- 1-( 3'-deoxy-fi-~-lyxopyranosyl)uracil (4d) and 1-(3'-Anilino-3'-deoxy-~-~ -lyxofuranosyl)uracil(5a). A mixture of 3f (300 mg, 1.0 mmol), 6 N NaOH (3.8 mL), and EtOH (3.8 mL) was heated at 75-80 “C strictly as for the above cases. TLC-monitoring showed that an extremely mobile sub- stance was forming together with the anticipated, slightly less ...