Synthesis, spectroscopic characterization, X-ray structure, and in vivo neurotropic activity of new 1, 5-benzodiazepin-2-ones

AA Gaponov, ET Zlenko, SV Shishkina…

文献索引：El-Shafei, A. K.; El-Kashef, H. S.; El-Khawaga, A. M. Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 7 p. 655 - 657

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摘要

... Experimental methods. Chemistry. ... Yield: method A, 0.88 g (93 %); mp 28–29 °C (28 °C (El-Shafei et al., 1982)); IR (KBr) cm −1 : 1670, 1610, 1585; 1 H NMR (500 MHz, DMSO-d 6 ): 2.30 (s, 3H, C–CH 3 ), 2.76 (d, 1H, J = 11.4, CH 2 ), 3.28 (d, 1H, J = 11.8, CH 2 ), 3.30 (s, 3H ...