Improved synthesis of dialkylthioxaphosphoranesulfenyl chlorides and bromides

A Łopusiński, L Łuczak, J Michalski

文献索引：Lopusinski, A.; Luczak, L.; Michalski, J. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 40, p. 233 - 236

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被引用次数: 2

摘要

Abstract Dialkylthioxaphosphoranesulfenyl chlorides and bromides can be conveniently prepared in the reaction of the corresponding thioamides with hydrogen chloride generated in situ with trimethylsilyl chloride and ethanol. Stability of the chlorides and bromides obtained by this method is high and the yields are quantitative.