Journal of the American Chemical Society

4, 4'-Tetramethyldiaminodiphenyl Ether

GA Reynolds

文献索引：Reynolds Journal of the American Chemical Society, 1951 , vol. 73, p. 4996

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被引用次数: 11

摘要

prepared in the following manner: Commercially available 4, 4'-dinitrodiphenyl ether was reduced, using Raney nickel catalyst, to give the corresponding diamine. Alkylation of the diamine with methyl iodide yielded tetramethyldiaminodiphenyl ether melting at 61-62'. The product formed a picrate which melted at 174-175'. Holzmann'prepared this compound by heating an alcoholic solution of 4, 4'-tetramethyldiarninodiphenyl sulfide with two ...