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New Method of Synthesis of 5-Acetyl-3-cyano-6-methylpyridine-2 (1H)-Thione and Its Properties

YY Yakunin, VD Dyachenko, VP Litvinov

文献索引:Yakunin; Dyachenko; Litvinov Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 581 - 587

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被引用次数: 5

摘要

Abstract 5-Acetyl-3-cyano-6-methylpyridine-2 (1H)-thione was obtained by the reaction of ethoxymethyleneacetylacetone with cyanothioacetamide in the presence of N- methylmorpholine. Its alkylation, bromination of the 2-methylthio derivative, and the