Syntheses and structure of 8-, 7-, and 6-membered silacycloallenes

…, SA Petrich, VG Young Jr, MS Gordon…

文献索引：Pang, Yi; Petrich, Scott A.; Young, Victor G.; Gordon, Mark S.; Barton, Thomas J. Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2534 - 2536

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被引用次数: 39

摘要

0 0 2 4 6 8 10 12 14 Glucose concentration (mM) Figure 3. Calibration curve of the glucose biosensor (taken at 700 mV vs SCE). The following molding procedure was used in order to entrap glucose oxidase in the vanadium oxide matrix. First, 3 g of vanadium pentaoxide (BDH) was fused at 850 OC for 3 h (to increase the V4+/V5+ ratio), and it was then quenched in 5 mL of distilled water, forming dark brown vanadium pentaoxide gel. Approximately 1 g of the gel was ...