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Synthetic communications

Practical Sulfonylation of Amines with 4??Hydroxybenzenesulfonyl Chloride: In Situ Silylation–Desilylation

JI Levin, MT Du, K Park

文献索引:Levin, Jeremy I.; Du, Mila T.; Park, Kaapjoo Synthetic Communications, 2004 , vol. 34, # 15 p. 2773 - 2781

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被引用次数: 5

摘要

A one??pot procedure for the efficient sulfonylation of amines with 4??hydroxybenzenesulfonyl chloride involving in situ protection and deprotection of the phenol with N,O??bis(trimethylsilyl) acetamide (BTSA) is presented. ... A one??pot procedure for the efficient sulfonylation of amines with 4??hydroxybenzenesulfonyl chloride involving in situ protection and deprotection of the phenol with N,O??bis(trimethylsilyl)acetamide (BTSA) is presented. ... View all references we ...