Synthesis, spectroscopic studies, and X-ray crystal structure of N-heteryliminophosphoranes

…, MA Al-Jaradah, KA Al-Farhan, AA Mousa

文献索引：Alkhathlan; Al-Jaradah; Al-Farhan; Mousa Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 2 p. 373 - 388

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被引用次数: 10

摘要

N-[2-(α-Bromoacetyl) phenyl] imides (prepared in two steps from 2-aminoacetophenone) gave, upon treatment with sodium azide, fused azidoquinolines via an intramolecular cyclization. Reaction of the above azides with phosphines gave N- heteryliminophosphoranes. The IR, 1H-, 13C-, and 31P-NMR and MS spectra of these compounds as well as the x-ray crystal structure of two of them is reported.