... Pharmazie 65 (2010) 3 163 Page 3. ... acid in the ratio of 100:0.05 (v/v) as a mobile phase - A and acetonitrile: trifluoroacetic acid in the ratio of 100:0.05 (v/v) as a mobile phase - B using the following gra- dient/elution (T/%B: 0/10, 12/62,16/65,17/10 ... The injected volume was 10 μL. ...
[Tanis, Steven P.; Parker, Timothy T.; Colca, Jerry R.; Fisher, Roberta M.; Kletzein, Rolf F. Journal of Medicinal Chemistry, 1996 , vol. 39, # 26 p. 5053 - 5063]