Mild oxidation of alkyl halides to aldehyde derivatives

JB Hendrickson, DD Sternbach

文献索引：Hendrickson,J.B.; Sternbach,D.D. Journal of Organic Chemistry, 1975 , vol. 40, p. 3450 - 3452

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被引用次数: 19

摘要

Organometallic reagents were manipulated using standard procedure~.~~ GLC analyses were carried out using an F & M Model 810 instrument and flame ionization detection, by unexceptional internal standard techniques. Butane and butene analyses utilized a 3-ft 3% Apiezon on alumina column; other analyses utilized an 8-ft 20% UC-W98 silicone rubber on Chromosorb P column. n-Hexane was purified by distillation under nitrogen from a ...