前往化源商城

Synthesis of tetrachloroisophthalic and-terephthalic aldehydes and stable bis (nitrile oxides) based on them

LI Belen'kii, GP Gromova, BV Lichitskii…

文献索引:Belen'kii; Gromova; Lichitskii; Krayushkin Russian Chemical Bulletin, 1997 , vol. 46, # 1 p. 101 - 104

全文:HTML全文

被引用次数: 1

摘要

Abstract A new route for the synthesis of 2, 4, 5, 6-tetrachloroisophthalic and 2, 3, 5, 6- tetrachloroterephthalic aldehydes from the corresponding tetrachlorobenzenes was developed. The method involves dichloromethylation of the initial compounds with chloroform in the presence of aluminum chloride and subsequent hydrolysis of the resulting 1, 3-bis (dichloromethyl)-2, 4, 5, 6-tetrachlorobenzene and 1, 4-bis (dichloromethyl)-2, 3, 5 ...