... splitting, the C-6 signal is split with 10.8 and 1.3Hz), the C-5 resonance shows two ... discriminated employing 2D (δ,J) long-range INEPT spectra with selective excitation[11] of the resonances due to H ... C-5 and C-6 (δ C-5 > δ C-6). However, these differences in chemical shifts are ...