Abstract Tertiary 5-nitrofurylamines were prepared by a nucleophilic substitution of 5-nitro-2- furfuryl bromide (I) with aliphatic secondary amines. According to reaction conditions N-(5- nitro-2-furfuryl)-X-phenylamines or their mixture with N, N-di (5-nitro-2-furfuryl)-X- phenylamines were obtained from the reaction of I with substituted primary aromatic amines. Compound I gave with 2-aminophenol a mixture of O-and N-mono-and disubstituted ...