Derivatives of coumaran. VI. Reduction of 2-acetobenzofuran and its derivatives

RL Shriner, J Anderson

文献索引：Shriner; Anderson Journal of the American Chemical Society, 1939 , vol. 61, p. 2705,2706

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被引用次数: 30

摘要

Oct., 1939 REDUCTION OF 2-ACETOBENZOFURAN AND ITS DERIVATIVES ... Diethylcyclohexylamine was prepared from cyclo- hexylamine and diethyl sulfate. Primary and secondary amines were removed with benzenesulfonyl chloride. The product boiled at 68.5-69 at 10 mm.; neut. equiv. calcd. 155.3, found 166.1. Cyclohexanol was prepared from diethylcyclohexyl- amine in 33% yield under the conditions used for the hydrolysis of cyclohexylamine. ...