Zur Kenntnis der Reaktionsfähigkeit des Thiomorpholins und alkylsubstituierter Thiomorpholine, 4. Mitt.

F Asinger, A Saus, M von Wachtendonk

文献索引：Asinger, Friedrich; Saus, Alfons; Wachtendonk, Magdalena von Monatshefte fuer Chemie, 1980 , vol. 111, p. 385 - 398

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摘要

Abstract Thiomorpholine as well as alkyl substituted thiomorpholines and their Sdioxides, respectively, are transformed into the corresponding N-Aminothiomorpholines by nitrosation (1–5) followed by the reduction with zinc in acetic acid/acetic acid anhydride under simultaneous formation of the corresponding N-acetyl derivates, and hydrolysis by hydrochloric acid (6–9). Examples of this method are described. 4-Aminothiomorpholines ...