The Journal of Organic Chemistry

An investigation of the mode of formation of the 10-P-5 protonated phosphatrane [cyclic] HP (OCH2CH2) 3N+

LE Carpenter, JG Verkade

文献索引：Carpenter, L. E.; Verkade, J. G. Journal of Organic Chemistry, 1986 , vol. 51, # 22 p. 4287 - 4288

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被引用次数: 8

摘要

Me4Si) 1.00 (3 H, t, J = 7.3 Hz), 1.54 (3 H, s), 1.90 (2 H, q, J = 7.3 Hz), 8.05 (1 H, d, J = 9.6 Hz), 8.38 (1 H, dd, J = 9.6 Hz, J = 2.4 Hz), 9.08 (1 H, d, J = 2.4 H), 14.09 (1 H, s) ppm; 13C NMR (MezSO-d6, Me4&) 7.38, 23.72,31.93,85.56, 115.57,122.60,130.02, 130.14, 138.29, 143.82, 149.00, 158.22 ppm; mass spectrum, m/e (relative intensity) 323 (M', 19), 294 (lOO), 273 (24), 183 (21). Anal. Calcd for CI2Hl3N5o6: C, 44.59; H, 4.05; N, 21.66. Found: C, 44.66; ...