… , propionate and butyrate in plasma: determination of the concentration and isotopic enrichment by gas chromatography/mass spectrometry with positive chemical …
E Pouteau, I Meirim, S Métairon…
文献索引：Pouteau, Etienne; Meirim, Isabelle; Metairon, Sylviane; Fay, Laurent-Bernard Journal of Mass Spectrometry, 2001 , vol. 36, # 7 p. 798 - 805
Abstract This study describes a rapid and simple method to determine short-chain fatty acid (SCFA) concentrations and their isotopic enrichments (M 0+ 1 and M 0+ 2) in human plasma. Sample preparation involves SCFA extraction and derivatization with 1-(tert- butyldimethylsilyl) imidazole. Gas chromatography/mass spectrometry was performed using chemical ionization with ammonia as the reagent gas. Outstanding resolution, excellent ...
