The Journal of Organic Chemistry

Reaction of Furan-Based o-Quinodimethanes with Triplet Oxygen. Formation of Cyclic Peroxides, 1

CH Chou, WS Trahanovsky

文献索引：Chou, Chin-Hsing; Trahanovsky, Walter S. Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5449 - 5451

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被引用次数: 23

摘要

Results The flash vacuum pyrolysis (FVP) of (5-tert-butyl-2-methyl-3-fury1) methyl benzoate (4c) at 550-560" C and ca. Torr produced a white product band in the cold trap which was cooled to-196 0C. 7 A 1: l mixture of CS2 and CDCl3 was added to the trap, and the product mixture was allowed to warm to-78" C. The IH NMR spectrum of the product mixture recorded at-60" C