Oxidative chlorination of [U??14C] phenol

D Georgin, S de Suzzoni??Dezard…

文献索引：Georgin; De Suzzoni-Dezard; Noel Journal of Labelled Compounds and Radiopharmaceuticals, 1996 , vol. 38, # 7 p. 645 - 649

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被引用次数: 1

摘要

The preparation of [U- 14 C] 2,4-dichlorophenol was formerly achieved by a Sandmeyer reaction with [U- 14 C] 2,4-dichloroaniline but this sensitive step gave unreproductive yields in our hands. ... We describe another route to [U- 14 C] 2,4-dichlorophenol by the oxidative chlorination of [U- 14 C] phenol. This shorter route is safer and gives satisfactory yields. The nature of the oxidizer is discussed. ... Copyright © 1999-2015 John Wiley & Sons, Inc. All Rights ...