Azo group-assisted nucleophilic aromatic substitutions in haloarene derivatives: preparation of substituted 1-iodo-2, 6-bispropylthiobenzenes

…, VC McKenzie, P Kaszynski

文献索引：Garst, Michael E.; Lukton, David Synthetic Communications, 1980 , vol. 10, # 2 p. 155 - 160

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被引用次数: 13

摘要

... free heterocyclic radicals 1,2 required 3 4-substituted 1-iodo-2,6-bis(propylthio)benzenes 1 as synthetic intermediates. ... Calcd for C 10 H 10 Cl 2 S: C, 45.30; H, 3.80. ... The volume of THF was reduced, and the mixture was poured into water and extracted (CH 2 Cl 2 /hexanes, 1:7 ...