... The olefin, therefore, had the regio- and stereo- chemistry shown in 7. In addition, the olefinic protons ... The combined organic extracts were dried and concentrated and the residue was purified by flash chromatography ... 3.51 (3 H, s, CHSd or CH34, 3.55 (1 H, d, J = 7 Hz, He), 3.68 ...